SUPEREX F-500
Supercritical Extraction System
- SuperEx high-pressure gas booster pump (in-house production specifically for the equipment)
- 500 ml extraction vessel
- Working pressure up to 345 bar
- Working temperature up to 90 °C
- CO2 pre-cooling/liquefaction unit
- Extraction in continuous (dynamic) CO2 flow mode
- Temperature control via PID algorithm
- Fully automatic digital pressure control
- Additional pump for co-solvent (up to 30 ± 1 ml min-1)
- Easy loading of samples thanks to fabric (polyester) loading bags
- Reversible flow direction for liquid raw materials
- Possibility of collecting extract directly in 50 ml centrifuge tubes
- Liquid trap function in a 50 ml secondary trap
- Independent electronic and mechanical overpressure protection system
- All contact surfaces made of stainless steel 316
- The ground and polished inner surface of the extractor prevents microbial and bacterial activity
- Co-solvent feed pump (30±1 ml/min)
- Increase in maximum working pressure to 700 bar
- Increase in working temperature to 200 °C
- Monitoring of volumetric flow rate of CO2 after pressure release (L min-1). An automatic backpressure regulator with digital and analog flow rate control is installed.
- Function of monitoring the mass of the extract in real time and automatic plotting of the extraction curve
- Module for raw material impregnation/impregnation. This module includes a second high-pressure reservoir (250 ml) and a cyclic pump that ensures continuous circulation of supercritical CO2 through both reservoirs. The 250 ml vessel contains a liquid reagent, solution or other component soluble in supercritical CO2, which is to be transferred to the substrate included in the main 500 ml vessel. CO2 is first pumped into the smaller vessel and allows the impregnation material to dissolve. The valves between the two vessels are then opened and the CO2 pump is turned on to equalize the pressure to the set value. The cyclic pump is then started, which continuously circulates the dissolved impregnating material through the substrate
- Micronization module. The micronization module includes a pump for taking liquid with an adjustable volumetric flow rate, a steel basket collector for collecting microparticles, and a coaxial nozzle installed inside the collector. The coaxial flow of supercritical CO2 acts as an antisolvent and causes the precipitation of components of the sample solution, poorly soluble in CO2, from a fine aerosol into microparticles
- Coriolis flowmeter Bass Instruments (Turkey)
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F-500.Video
SUPEREX F-500*
Supercritical Impregnation Module
- SuperEx high pressure gas booster pump (in-house production specifically for the equipment)
- 500 ml extraction vessel
- Working pressure up to 345 bar (possible to increase to 700 bar)
- Working temperature up to 90 °C (possible to increase to 200 °C)
- CO2 pre-cooling/liquefaction unit
- Feedstock impregnation/impregnation module: This module includes a second high pressure vessel (250 ml) and a cyclic pump that ensures continuous circulation of supercritical CO2 through both vessels. The 250 ml vessel contains a liquid reagent, solution or other component soluble in supercritical CO2, which is to be transferred to the substrate included in the main 500 ml vessel. CO2 is first pumped into the smaller vessel and allows the impregnation material to dissolve. The valves between the two vessels are then opened and the CO2 pump is turned on to equalize the pressure to the set point. The cyclic pump is then started, which continuously circulates the dissolved impregnating material through the substrate.
- Extraction in continuous (dynamic) CO2 flow mode
- Temperature control using PID algorithm
- Fully automatic digital pressure control
- Additional pump for co-solvent (up to 30 ± 1 ml min-1)
- Easy loading of samples thanks to fabric (polyester) loading bags
- Variable flow direction for liquid raw materials
- Possibility of collecting extract directly into 50 ml centrifuge tubes
- Liquid trap function in a 50 ml secondary trap
- Independent electronic and mechanical overpressure protection system
- All contact surfaces are made of 316 stainless steel
- Ground and polished inner surface of the extractor prevents microbial and bacterial activity
- Increase in maximum working pressure to 700 bar
- Increase in working temperature to 200 °C
- Monitoring of volumetric flow rate of CO2 after pressure release (L min-1). An automatic backpressure regulator with digital and analog flow rate control is installed.
- Module for feed impregnation/impregnation. This module includes a second high-pressure vessel (250 ml) and a cyclic pump that ensures continuous circulation of supercritical CO2 through both vessels. The 250 ml vessel contains a liquid reagent, solution or other component soluble in supercritical CO2, which is to be transferred to the substrate included in the main 500 ml vessel. CO2 is first pumped into the smaller vessel and allows the impregnating material to dissolve. Then the valves between the two vessels are opened and the CO2 pump is turned on to equalize the pressure to the set value. A cyclic pump is then started, which continuously circulates the dissolved impregnating material through the substrate
- Micronization module. The micronization module includes a pump for collecting liquid with an adjustable volumetric flow rate, a steel basket-collector for collecting microparticles, and a coaxial nozzle installed inside the collector. Coaxial flow of supercritical CO2 acts as an antisolvent and causes precipitation of sample solution components poorly soluble in CO2 from a fine aerosol into microparticles
- Coriolis flowmeter Bass Instruments (Turkey)
- single- or multi-tier holders/reservoirs for substrate and/or impregnating material
UPON REQUEST OF THE CUSTOMER WE PRODUCE UNITS WITH A MODULE OF SUPERCRITICAL IMPREGNATION OF RAW MATERIALS (IMPREGNATION) UP TO INDUSTRIAL VOLUMES (EXTRACTOR VOLUME UP TO 100 L, HIGH-PRESSURE TANK VOLUME UP TO 50 L)
More details about the SuperEx unit with a raw material impregnation/impregnation module, technologies and areas of application can be found here
More details about the SuperEx unit with a raw material impregnation/impregnation module, technologies and areas of application can be found here
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SUPEREX SC-500
Supercritical Extraction System
- SuperEx high pressure gas booster pump (in-house production specifically for the equipment). CO2 flow rate 100 ml min-1
- 500 ml extraction vessel
- 2 x 150 ml separators with temperature and pressure control up to 220 bar
- CO2 cooling/liquefaction system for effective pressure boosting
- Working pressure up to 345 bar
- Working temperature up to 90 °C
- All contact surfaces are made of 316 stainless steel
- Ground and polished extractors and separators prevent microbial and bacterial activity
- Temperature control using PID algorithm
- Automation system. The unit has a control panel that allows you to control and monitor all conditions of pressure, temperature, solvent and co-solvent supply, pressure reduction and CO2 recirculation. The system is equipped with special software for starting and stopping (including emergency shutdown) static and dynamic extraction modes
- Automatic back pressure regulators (BPR)
- Stainless steel or cotton baskets for easy loading of raw materials
- Cyclone flow function for all separators ensures effective removal of dissolved compounds from scCO2
- Liquid traps (with water and/or solvents) can be included in the separators to capture dissolved compounds
- Average energy consumption: 5 kWh
- Average CO2 consumption: ≤150 g per working cycle (CO2 recirculation 90–95%)
- Increase of maximum pressure to 700 bar (test pressure 1050 bar)
- Increase of working temperature to 200 °C
- Additional 0.5 L extraction vessel
- Additional 150 ml separator with adjustable pressure
- Automatic back pressure regulators (BPR)
- Activated carbon and silica gel (or molecular sieve) filters on the recirculation line
- Electro-pneumatic system for adjusting the CO2 flow rate
- Cooling package of the first and last separators (optional) to -10 °C
- Feed impregnation/impregnation module. This module includes a second high-pressure tank (250 ml) and a cyclic pump that ensures continuous circulation of supercritical CO2 through both tanks. The 250 ml vessel contains a liquid reagent, solution or other component soluble in supercritical CO2, which must be transferred to the substrate included in the main 500 ml vessel. CO2 is first pumped into the smaller vessel and allows the impregnating material to dissolve. Then the valves between the two vessels are opened and the CO2 pump is turned on to equalize the pressure to the set value. Then the cyclic pump is started, which continuously circulates the dissolved impregnating material through the substrate
- Micronization module. The micronization module includes a pump for liquid intake with an adjustable volumetric flow rate, a steel basket collector for collecting microparticles, and a coaxial nozzle installed inside the collector. The coaxial flow of supercritical CO2 acts as an antisolvent and causes the precipitation of components of the sample solution, poorly soluble in CO2, from a fine aerosol into microparticles
- Bass Instruments Coriolis Flow Meter
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SUPEREX F-1000
Supercritical Countercurrent Extraction System
- 1L extraction vessel
- Additional 0.5L extraction column
- CO2 liquefaction system for efficient pressure increase
- Working pressure up to 345 bar
- Working temperature up to 70 °C
- All contact surfaces are made of 316 stainless steel
- Ground and polished extractors and separators prevent microbial and bacterial activity
- Special design for counter-current extraction of liquid raw materials
- Additional pump for feeding co-solvent and liquid raw materials
- Possibility of real-time flow rate monitoring
- Temperature control using PID algorithm
- Digital fully automatic pressure control
- Convenient sample loading
- Independent electronic and mechanical overpressure protection systems
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F-1000.Video
SUPEREX SC-1000
Supercritical Extraction System
- SuperEx high pressure gas booster pump (in-house production specifically for the equipment). CO2 flow rate 100 ml min-1
- 1 L extraction vessel
- 2 x 300 ml separators with temperature and pressure control up to 220 bar
- CO2 cooling/liquefaction system for effective pressure boosting
- Working pressure up to 345 bar
- Working temperature up to 90 °C
- All contact surfaces are made of 316 stainless steel
- Ground and polished extractors and separators prevent microbial and bacterial activity
- Temperature control using PID algorithm
- Automation system. The unit has a control panel that allows you to control and monitor all conditions of pressure, temperature, solvent and co-solvent supply, pressure reduction and CO2 recirculation. The system is equipped with special software for starting and stopping (including emergency shutdown) static and dynamic extraction modes
- Automatic back pressure regulators (BPR)
- Stainless steel or cotton baskets for easy loading of raw materials
- Cyclone flow function for all separators ensures effective removal of dissolved compounds from scCO2
- Liquid traps (with water and/or solvents) can be included in the separators to capture dissolved compounds
- Average energy consumption: 5 kWh
- Average CO2 consumption: ≤150 g per working cycle (CO2 recirculation 90–95%)
- Increase of maximum pressure to 700 bar (test pressure 1050 bar)
- Increase of working temperature to 200 °C
- Additional extraction vessel (0.5 L or 1 L)
- Additional 300 ml separator with adjustable pressure
- Automatic regulators Back Pressure Relief (BPR)
- Activated carbon and silica gel (or molecular sieve) filters in the recirculation line
- Electro-pneumatic system for adjusting the CO2 flow rate
- Cooling package for the first and last separators (optional) down to -10 °C
- Feed impregnation/wet impregnation module. This module includes a second high-pressure vessel (500 ml) and a cyclic pump that ensures continuous circulation of supercritical CO2 through both vessels. The 500 ml vessel contains a liquid reagent, solution or other component soluble in supercritical CO2 that needs to be transferred to a substrate included in the main 1 L vessel. CO2 is first pumped into the smaller vessel and allows the impregnating material to dissolve. Then the valves between the two vessels are opened and the CO2 pump is turned on to equalize the pressure to the set value. A cyclic pump is then started, which continuously circulates the dissolved impregnating material through the substrate
- Micronization module. The micronization module includes a pump for liquid intake with an adjustable volumetric flow rate, a steel basket collector for collecting microparticles, and a coaxial nozzle installed inside the collector. The coaxial flow of supercritical CO2 acts as an antisolvent and causes the precipitation of components of the sample solution, poorly soluble in CO2, from a fine aerosol into microparticles
- Bass Instruments Coriolis flow meter
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SUPEREX SC-2000
Supercritical Extraction System
- SuperEx high pressure gas booster pump (in-house production specifically for the equipment). CO2 flow rate 200 ml min-1
- 2 L extraction vessel
- 2 x 500 ml separators with temperature and pressure control up to 220 bar
- CO2 cooling/liquefaction system for effective pressure boosting
- Working pressure up to 345 bar
- Working temperature up to 90 °C
- All contact surfaces are made of 316 stainless steel
- Ground and polished extractors and separators prevent microbial and bacterial activity
- Temperature control using PID algorithm
- Automation system. The unit has a control panel that allows you to control and monitor all conditions of pressure, temperature, solvent and co-solvent supply, pressure reduction and CO2 recirculation. The system is equipped with special software for starting and stopping (including emergency shutdown) static and dynamic extraction modes
- Automatic back pressure regulators (BPR)
- Stainless steel or cotton baskets for easy loading of raw materials
- Cyclone flow function for all separators ensures effective removal of dissolved compounds from scCO2
- Liquid traps (with water and/or solvents) can be included in the separators to capture dissolved compounds
- Average energy consumption: 5 kWh
- Average CO2 consumption: ≤260 g per working cycle (CO2 recirculation 90–95%)
- Increase of maximum pressure to 700 bar (test pressure 1050 bar)
- Increase of working temperature to 200 °C
- Additional extraction vessel (0.5 L - 2 L)
- Additional 500 ml separator with adjustable pressure
- Automatic regulators back pressure (BPR)
- Filters with activated carbon and silica gel (or molecular sieve) on the recirculation line
- Electropneumatic system for adjusting the CO2 flow rate
- Cooling package for the first and last separators (optional) to -10 °C
- Coriolis flow meter Bass Instruments
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SUPEREX SC-3000
Supercritical Extraction System
- High pressure gas booster pump SuperEx (in-house production specifically for the equipment). CO2 flow rate 300 ml min-1
- Extraction vessel with a volume of 3 L
- 2 separators of 750 ml with temperature and pressure control up to 220 bar
- CO2 cooling / liquefaction system for effective pressure increase
- Working pressure up to 345 bar
- Working temperature up to 90 °C
- All contact surfaces are made of stainless steel 316
- Ground and polished extractors and separators prevent microbial and bacterial activity
- Temperature control using a PID algorithm
- Automation system. The unit has a control panel that allows you to control and monitor all conditions of pressure, temperature, solvent and co-solvent supply, pressure reduction and CO2 recirculation. The system is equipped with special software for starting and stopping (including emergency shutdown) static and dynamic extraction modes
- Automatic back pressure regulators (BPR)
- Stainless steel or cotton baskets for easy loading of raw materials
- Cyclone flow function for all separators ensures effective removal of dissolved compounds from scCO2
- Liquid traps (with water and/or solvents) can be included in the separators to capture dissolved compounds
- Average energy consumption: 5 kWh
- Average CO2 consumption: ≤390 g per working cycle (CO2 recirculation 90–95%)
- Increase of maximum pressure to 700 bar (test pressure 1050 bar)
- Increase of working temperature to 200 °C
- Additional extraction vessel (0.5 L - 3 L)
- Additional 750 ml separator with adjustable pressure
- Automatic regulators back pressure (BPR)
- Filters with activated carbon and silica gel (or molecular sieve) on the recirculation line
- Electro-pneumatic system for adjusting the CO2 flow rate
- Cooling package of the first and last separators (at the operator's choice) to -10 °C
- Coriolis flow meter Bass Instruments
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SUPEREX SC-4000
Supercritical Extraction System
- SuperEx high pressure gas booster pump (in-house production specifically for the equipment). CO2 flow rate 400 ml min-1
- 4 L extraction vessel
- 2 x 1 L separators with temperature and pressure control up to 220 bar
- CO2 cooling/liquefaction system for effective pressure boosting
- Working pressure up to 345 bar
- Working temperature up to 90 °C
- All contact surfaces are made of 316 stainless steel
- Ground and polished extractors and separators prevent microbial and bacterial activity
- Temperature control using PID algorithm
- Automation system. The unit has a control panel that allows you to control and monitor all conditions of pressure, temperature, solvent and co-solvent supply, pressure reduction and CO2 recirculation. The system is equipped with special software for starting and stopping (including emergency shutdown) static and dynamic extraction modes
- Automatic back pressure regulators (BPR)
- Stainless steel or cotton baskets for easy loading of raw materials
- Cyclone flow function for all separators ensures effective removal of dissolved compounds from scCO2
- Liquid traps (with water and/or solvents) can be included in the separators to capture dissolved compounds
- Average energy consumption: 6 kWh
- Average CO2 consumption: ≤520 g per working cycle (CO2 recirculation 90–95%)
- Increase of maximum pressure to 700 bar (test pressure 1050 bar)
- Increase of working temperature to 200 °C
- Additional extraction vessel (0.5 L - 5 L)
- Additional 2L separator with adjustable pressure
- Automatic back pressure regulators pressure (BPR)
- Filters with activated carbon and silica gel (or molecular sieve) on the recirculation line
- Electropneumatic system for regulating the CO2 flow rate
- Cooling package of the first and last separators (at the operator's choice) to -10 °C
- Coriolis flow meter Bass Instruments
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SUPEREX SC-5000
Система Сверхкритической Экстракции
- High pressure gas booster pump SuperEx (in-house production specifically for the equipment). CO2 flow rate 500 ml min-1
- Extraction vessel with a volume of 5 L
- 2 separators of 2 L with temperature and pressure control up to 220 bar
- CO2 cooling/liquefaction system for effective pressure increase
- Working pressure up to 345 bar
- Working temperature up to 90 °C
- All contact surfaces are made of stainless steel 316
- Ground and polished extractors and separators prevent microbial and bacterial activity
- Temperature control using a PID algorithm
- Automation system. The unit has a control panel that allows you to control and monitor all conditions of pressure, temperature, solvent and co-solvent supply, pressure reduction and CO2 recirculation. The system is equipped with special software for starting and stopping (including emergency shutdown) static and dynamic extraction modes
- Automatic back pressure regulators (BPR)
- Stainless steel or cotton baskets for easy loading of raw materials
- Cyclone flow function for all separators ensures effective removal of dissolved compounds from scCO2
- Liquid traps (with water and/or solvents) can be included in the separators to capture dissolved compounds
- Average energy consumption: 6 kWh
- Average CO2 consumption: ≤650 g per working cycle (CO2 recirculation 90–95%)
- Increase of maximum pressure to 700 bar (test pressure 1050 bar)
- Increase of working temperature to 200 °C
- Additional extraction vessel (0.5 L - 5 L)
- Additional 2L separator with adjustable pressure
- Automatic back pressure regulators pressure (BPR)
- Filters with activated carbon and silica gel (or molecular sieve) on the recirculation line
- Electropneumatic system for regulating the CO2 flow rate
- Cooling package of the first and last separators (at the operator's choice) to -10 °C
- Coriolis flow meter Bass Instruments
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